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Kemphos-822 (Self Accelerated Wire Drawing Zinc Phosphating Chemical) (Self acclerated wire drawing
zinc phosphating chemical)
Product Description Kemphos-822 is a heavy zinc phosphate compound which produces
excellent zinc/iron phosphate coating on Iron and steel supplementary
finishes. This product does not accelerator addition in the bath
periodically. The conversion coating produced with Kemphos-822, when
used in conjunction with suitable lubricant, reduces friction under
low medium and high carbon forming on steel, cold shaping, drawing of
wire. Lubricants and drawing compounds become firmly anchored to the
phosphate coating for improved drawing.
Product Specifications
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a.
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Colour
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Light Green liquid
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b.
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Chemical Composition
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Blend of zinc & Nickel metal phosphates,
Nitrates and additives
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c.
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Odour
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Slightly Pungent
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d.
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Foaming Tendency
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Nil
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e.
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Reliability
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Good
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f.
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Handling
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Avoid Skin Contact
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g.
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Solubility
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Good
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h.
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pH
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Acidic range
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I.
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Toxicity
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Nil
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j.
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Flash Point
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Nil
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k.
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Pollution Hazard
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Moderate
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I.
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Coating Weight
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8 -11gm/m2
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Product Operating Data
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Concentration
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3% by v/v
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Temperature
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70 - 80°c
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Time
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7 -15 min
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T.A.
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20 25 ml (3%
solution)
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F.A.
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4 4.5 ml (3%
solution)
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Acid Ratio
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5.0 5.5
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Product Operating Procedure
Pickling Pickling should be carried out
either in sulphuric or hydrochloric acid, in combination with
suitable acid inhibitors in sufficient strength to remove rust and
scale present on the work.
Rinsing The stage rinsing should be followed
after pickling process, first rinse with cold water and finally
rinsed with jet pressure. The rinsing tank should be cleaned
regularly.
Fill the tank 2/3 with water and add
recommended qty. of Khemphos-822. Fill th tank to the operating level
with water and mix thoroughly. There for total acid and if necessary
and enough Kemphos-822 to bring total acid to operating level and mix
thoroughly. After phosphating with Kemphos-822, the work should be
rinsed with continuous flowing water and subsequently once again
rinsed in hot neutralizing and dried. The neutralizing solution is
made up with 0.1 kg. Of soda ash per 100 litres of bath.
Operating
Recommendation Proper rinsing is very much
essential after pickling in mineral acids in order to remove residues
from the surface of the work. Any carry over of the acid to the
phosphating tank will lead to excessive sludge formation
deterioration of phosphate coating and high chemical cost.
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Proper control of temperature,
pointage and time minimise the chemical consumption.
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Thin coating may result from a low bath temperature and insufficient
treating time.
Product Application Equipments Kemphos-822 tank should be
fabricated with 3 to 4 mm thick M.S. Plates with continuous
convection current hating system.
6.0
Testing and Control Procedure The Kemphos-822 is controlled by
simple titration for total acids. Ferrous Iron concentration of
Kemphos-002 (Accelerator) by titration method.
Total
Acidity Pipette out 10 ml of bath solution into a beaker. Add 5 -10 drops of
indicator Phenolphthalein. Fill the burette to the zero mark and
titrate with N/10 sodium Hydroxide solution. Stir the solution until
pink colour appears. Note volume of N/10 sodium hydroxide solution
used.
Free Acidity Pipette out 10 ml. Of bath solution into a beaker. Add 5 -10 drops of
bromophenol blue Indicator. Fill the burette to the zero mark and
titrate with N/10 sodium hydroxide solution. Stir the solution until
blue violet colour appears. Note volume of N/0 sodium Hydroxide
solution used.
Chemical Replenishment Add 125 ml. Of Kemphos-822 per 100 ltrs. Bath for each point lacking.
The bath should be kept with in 1 ml. Of the specified titration
values.
During the processing sludge is formed and the same is accumulated in
the bottom of the tank. It should be removed at regular intervals.
Sludge removal is carried out by decanting the clear solution in a
emptied tank. Clean the phosphating tank and returned to the decanted
solution. The bath solution is resotred to is operating level by
adding water and chemical in the recommended proportion as used in
the original bath.
Safety Measures Kemphos-822 is an acidic liquid
material, and while handling proper care should be taken. Protect
eyes and skin by means of goggles, aprons, gloves, etc. If it comes in
contact with skin and eyes wash thoroughly with a flush of water and
get medical advice.
General Information Corrosion Resistance: Excellent Lubrication during wire drawing:
Excellent.
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